English

4

Not applicable.

Of all faculties

Improvement of knowledge of sampling, treatment of sample and final detection of harmful substances

Graduation in bachelor degree in the study program Protection of population at the Brno University of Technology or at similar study program at another university

Not applicable.

Teaching methods depend on the type of course unit as specified in the article 7 of BUT Rules for Studies and Examinations.

Oral examination, questions from all subjects discussed during lectures at this subject

1) Introduction, characteristic features of analytical methods application in the Integrated Rescue System
2) Sampling of gaseous samples (sampling bags, isolation of organic compounds using SPME, sorption tubes)
3) Sampling of liquid samples (waters, thinners, solvents, dyes, mercury)
4) Sampling of solid samples (soil, foods, biotic samples)
5) Sample treatment for detection of inorganic pollutants (dissolution, leaching, melting)
6) Methods of identification and determination of toxic inorganic elements and compounds (heavy metals, toxic anions): potentiometry, polarography, atomic absorption spectrometry
7) Sample treatment for detection of organic compounds (solid phase extraction, solid phase microextraction, liquid-liquid extraction, gas stripping, head-space analysis)
8) Methods of identification and determination of toxic organic compounds: Chromatographic separation methods
9) Methods of identification and determination of toxic organic compounds: IR spectrometry, UV-VIS spectrometry
10) Methods of identification and determination of toxic organic compounds: Mass spectrometry, hyphenated techniques
11) Mobile analytics methods for the on-site identification and determination of unknown compounds (PCHL-90, Merck Mobile Analytics)
12) Mobile analytical instrumentaion: Portable chromatographs, portable mass spectrometers
13) Special techniques for direct analysis of sample: DART, DESI, DAPCI

Not applicable.

Students will be introduced to basics of sampling of gaseous, liquid and silod samples including biotic ones, taking into account sampling of organic and inorganic compounds at various concentration levels. Further methods of sample treatment will be presented, mainly processes of target compounds isolation forma sample matrix, methods of sample clean-up and group fractionation, concentration techniques and basic derivatization reactions. The last topic will be the instrumental methods of the harmful substances identification and quantitation.

Students in full-time study form are checked within the range defined by the study program. For students in combined form the e-learning support is prepared covering all topics discussed in the full-time form. The knowledge obtained during the course is checked in final examination.

Not applicable.

Not applicable.

Klouda P.: Moderní analytické metody. Nakladatelství Pavel Klouda, 2003. (EN)
Janků J., Čermák J.: Vzorkování odpadů. Praha: VŠCHT, 2006. (EN)
Križan, V. Analýzy ovzduší. Alfa Bratislava, SNTL Praha, 1981 (EN)
Horáková M., Lischke P., Grünwald A.: Metody chemické analýzy vod. Praha: SNTL a Alfa, 1989 (EN)

Not applicable.

39 hours, optionally