Project detail

In-situ Synthesised Intermetallic Compounds in Kinetically Sprayed Deposits

Duration: 01.02.2013 — 31.12.2016

Funding resources

Czech Science Foundation - Standardní projekty

- whole funder (2013-02-01 - 2016-12-31)

On the project

Studie je zaměřena na získání poznatků a kontrolu tvorby intermetalických fází a jim odpovídajících mikrostruktur v práškovém depozitu připraveném kinetickým nanášením za studena a následným tepelným zpracováním. Ke splnění těchto cílů je nezbytné (i) zevrubně studovat proces depozice prostřednictvím kinetického nanášení za studena prášků vysoce reaktivních kovů (Ti, Al, Ni apod.) v porovnání s běžnými kompaktačními metodami a charakterizovat deformační texturu, mikrostrukturu a fázové složení depozitů; (ii) charakterizovat tyto parametry pro struktury získané tepelným zpracováním v běžné atmosféře, příp. v inertním plynu; (iii) rozvinout získané poznatky s cílem získat postup přípravy antioxidačních povlaků na experimentální TiAl slitině a (iv) kombinací získaných poznatků navrhnout postup přípravy materiálů s predikovatelnými vlastnostmi a dobrým aplikačním potenciálem.

Description in English
The study is aimed at gaining sufficient understanding and control over the formation of intermetallic phases and their respective microstructures in powder deposits prepared by cold gas dynamic spray technology and their subsequent thermal treatment. In order to pursue the aim there is a need for (i) a thorough study of the deposition process by cold gas dynamic spraying of highly reactive elements (Ti, Al, Ni etc.) in comparison with the traditional compacting methods and characterization of the deformation texture, microstructure and phase content of the deposits; (ii) characterization of these properties during heat treatment in ambient atmosphere or inert environment in order to allow controlling the microstructure and phase composition of the formed intermetallic materials; (iii) expanding of the obtained findings in order to develop a route for antioxidation coating formation in the experimental TiAl based alloy and (iv) combining of the gained knowledge in order to provide a defined path for creating materials with predictable qualities and good application potential.

Keywords
aluminidy titanu, intermetalické fáze, intermetalické slitiny, kinetické nanášení prášku za studena, depozice za studena, in situ reakce, kompozity, antioxidacní bariéry, objemová intermetalika

Key words in English
titanium; aluminides; intermetallic; compounds; intermetallic; alloys; cold; gas; dynamic; spray; cold; spray; in; situ; reactions; composites; antioxidation; bariers; bulk; intermetalics

Mark

GA13-35890S

Default language

Czech

People responsible

Dlouhý Ivo, prof. Ing., CSc. - principal person responsible

Units

Dept. of Mechanics and Design of Materials
- beneficiary (2013-02-01 - 2016-12-31)

Results

JAN, V.; ČÍŽEK, J. Cold Gas Dynamic Spraying of Bi-metallic Powders for Intermetallic Phases Formation. 6RIPT. 1. Limoges, Francie: 2013. p. 1-13. ISBN: 1.
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DLOUHÝ, I.; STRATIL, L.; FUKUTOMI, H.; HASEGAWA, M. Crack resistance characterization in TiAl intermetallics with enhanced toughness. Key Engineering Materials (print), 2016, vol. 741, no. 11, p. 13-18. ISSN: 1013-9826.
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MATLÁK, J. Možnosti využití elektronového paprsku ve strojírenských aplikacích. 2014.
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HANUSOVÁ, P.; NOVÁK, P. PREPARATION AND PROPERTIES OF Al – Fe AND Al – Fe – Cr ALLOYS. In METAL 2014 Conference Proceedings. 1. Ostrava: Tanger Ltd., Keltičkova 62, 710 00 Ostrava, 2014. p. 1249-1253. ISBN: 978-80-87294-54-3.
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ČÍŽEK, J.; MATĚJKOVÁ, M.; KAY, C.; KARTHIKEYAN, J.; KURODA, S.; KOVÁŘÍK, O.; SIEGL, J.; KHOR, K.; DLOUHÝ, I. Influence of Cold, Warm and Plasma Sprayed Layers on High-Cycle Fatigue Properties of Steel Specimens. In International Thermal Spray Conference 2014 Proceedings. Barcelona, Španělsko: DVS Media GmbH, 2014. p. 577-581. ISBN: 978-3-87155-574-9.
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ČÍŽEK, J.; MAN, O.; DLOUHÝ, I. Influence of Cold-Sprayed Al/Ti Deposition on High-temperature Oxidation and Mechanical Properties Deterioration of Ti-Al-Nb Intermetallic Substrates. In International Thermal Spray Conference 2014 Proceedings. Barcelona, Španělsko: DVS Media GmbH, 2014. p. 903-907. ISBN: 978-3-87155-574-9.
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JAN, V.; PÁLENÍKOVÁ, L.; ČUPERA, J.; ČÍŽEK, J. Formation of Intermetallic Phases in Fe-Al Binary Cold Spray Thick Deposit. In International Thermal Spray Conference 2014 Proceedings. Barcelona, Španělsko: DVS Media GmbH, 2014. p. 908-912. ISBN: 978-3-87155-574-9.
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ČÍŽEK, J.; DLOUHÝ, I.; ŠIŠKA, F.; KHOR, K. Modification of Plasma Sprayed TiO2 Coatings Characteristics via Controlling the In-flight Temperature and Velocity of the Powder Particles. JOURNAL OF THERMAL SPRAY TECHNOLOGY, 2014, vol. 23, no. 8, p. 1339-1349. ISSN: 1059-9630.
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ČUPERA, J.; JAN, V. Identification of phases in titanium alloy and correlation between EBSD, High Voltage, Medium Voltage and Low Voltage BSE imaging. 2014. p. 2940-2940.
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ČÍŽEK, J.; MAN, O.; ROUPCOVÁ, P.; LOKE, K.; DLOUHÝ, I. Oxidation Performance of Cold Spray Ti-Al Barrier Coated gamma-TiAl Intermetallic Substrates. Surface and Coatings Technology, 2015, vol. 268, no. 4, p. 85-89. ISSN: 0257-8972.
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MORAVČÍK, I.; PIŇOS, J.; ČÍŽEK, J.; DLOUHÝ, I. Mechanical Properties of Powder Deposits Compacted by Cold Spray Technology. SINTERING 2014. Nemecko: Sintering 2014, 2014. p. 308-308.
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HANUSOVÁ, P.; NOVÁK, P.; DLOUHÝ, I. Properties of Al – Fe – X alloys depending on the method of manufacturing. Lausanne: 2014.
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PÁLENÍKOVÁ, L.; JAN, V.; ČUPERA, J.; ČÍŽEK, J. MICROSTRUCTURE OF Fe-Al BINARY COLD SPRAY THICK DEPOSIT AFTER ANNEALING. In Metal 2014. 2014. p. 1328-1333. ISBN: 978-80-87294-52-9.
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JAN, V.; ČUPERA, J.; ČÍŽEK, J. On the search for producing intermetallics by diffusion reaction of cold spray bulk deposits. Surface and Coatings Technology, 2015, vol. 2015, no. 264, p. 216-223. ISSN: 0257-8972.
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ČÍŽEK, J.; MATĚJKOVÁ, M.; DLOUHÝ, I.; ŠIŠKA, F.; KAY, C.; KARTHIKEYAN, J.; KURODA, S.; KOVÁŘÍK, O.; SIEGL, J.; LOKE, K.; KHOR, K. Influence of Cold-Sprayed, Warm-Sprayed and Plasma Sprayed Layers Deposition on Fatigue Properties of Steel Specimens. JOURNAL OF THERMAL SPRAY TECHNOLOGY, 2015, vol. 24, no. 5, p. 758-768. ISSN: 1059-9630.
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MORAVČÍK, I.; ČÍŽEK, J.; DLOUHÝ, I. Preparation of high entropy alloy powders by mechano-chemical reactions. In MULTI-SCALE DESIGN OF ADVANCEDMATERIALS. Brno: Brno University of Technology, Antonínská 548/1, 601 90 Brno, 2015. p. 73-78. ISBN: 978-80-214-5146-9.
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HANUSOVÁ, P.; DLOUHÝ, I.; ČUPERA, J. PREPARATION OF Nb – Nb3Al/Al2O3 NANOCOMPOSITE POWDER BY MECHANO-CHEMICAL REACTION. In METAL 2015. Brno: Tanger Ltd., 2015. p. 320-325. ISBN: 978-80-87294-62-8.
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GAVENDOVÁ, P.; ČÍŽEK, J.; DLOUHÝ, I.; ČUPERA, J.; HANUSOVÁ, P. COMPARISON OF CoNiCrAlY COATINGS PRODUCED BY HVOF AND CGDS-SPRAYING TECHNIQUE. In METAL 2015. Brno: Tanger Ltd., 2015. p. 152-158. ISBN: 978-80-87294-62-8.
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GAVENDOVÁ, P.; DLOUHÝ, I.; ČÍŽEK, J.; ČUPERA, J.; HANUSOVÁ, P. Effect of electron beam remelting to microstructure and phase modification of HVOF and CGDS CoNiCrAlY coatings. In Heat Treatment and Surface Engineering from tradition to innovation. Italy: Associazione Italia di Metallurgia, 2015. p. 152-159. ISBN: 978-88-98990-03-0.
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MORAVČÍK, I.; ČÍŽEK, J.; DLOUHÝ, I. MULTICOMPONENT ALLOY POWDERS PREPARATION BY MECHANICAL ALLOYING. In METAL 2015. Brno: TANGER Ltd., 2015. p. 195-205. ISBN: 978-80-87294-62-8.
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ZELENÝ, M.; STRAKA, L.; SOZINOV, A. Ab initio study of Ni2MnGa under shear deformation. In ESOMAT 2015 – 10th European Symposium on Martensitic Transformations. MATEC Web of Conferences. EDP Sciences, 2015. p. 05006-1 (05006-6 p.)ISBN: 978-2-7598-1925-6. ISSN: 2261-236X.
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ZAPLETAL, J.; DOLEŽAL, P.; FINTOVÁ, S. STRUCTURE ANDMECHANICAL PROPERTIES OF QE22 MAGNESIUM ALLOY AND QE22 MAGNESIUM ALLOY BASED HYBRID COMPOSITE. Žilina: Žilinská univerzita, 2015. p. 1-5.
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MORAVČÍK, I.; ČÍŽEK, J.; HRYHA,E.; DLOUHÝ, I. Preparation of AlCoCrFeNiTi0.5 High Entropy Alloy by SPS from Mechanically Alloyed Powders. In EURO PM 2015 Proceedings. Reims France: European powder metallurgy association, 2015. p. 1-6. ISBN: 978-1-899072-47-7.
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MORAVČÍK, I.; ČÍŽEK, J.; GAVENDOVÁ, P.; DLOUHÝ, I. INFLUENCE OF SINTERING TEMPERATURE ON MICROSTRUCTURE AND MECHANICAL PROPERTIES OF HIGH ENTROPY ALLOY ALCOCRFENITI0,5. Konštrukčné materiály 2015. Žilina: Zilinská univerzita, 2015. p. 10-15.
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ČÍŽEK, J.; SEINER, H.; HUANG, R.; LANDA, M.; DLOUHÝ, I. Elastic Isotropy of Cold Sprayed Coatings. In International Thermal Spray Conference 2015 Proceedings. Long Beach, USA: ASM International, 2015. p. 353-356. ISBN: 978-1-62708-093-4.
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ČÍŽEK, J.; SEINER, H.; HUANG, R.; LANDA, M.; DLOUHÝ, I. Elastic Isotropy of Cold Sprayed Coatings. In International Conference of Engineering Against Failure. Skiathos, Řecko: University of Patras, 2015. p. 401-406. ISBN: 978-960-88104-5-7.
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ČÍŽEK, J.; SEINER, H.; HUANG, R.; LANDA, M.; DLOUHÝ, I. Elastic Isotropy of Cold Sprayed Coatings. Limoges: University of Limoges, 2015. p. 1-16.
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VÁLKA, L. The influence of impurity level on fracture behaviour of high strength structural steels. Žilina, Slovensko: Katedra materiálového inžinierstva, SF Žilinskej Univerzity v Žilině, 2015.
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JAN, V.; ČÍŽEK, J.; DYČKA, M.; ČUPERA, J. HYPO-EUTECTOID NITI ALLOY MANUFACTURED BY CGDS POWDER MIX DEPOSITION AND HEAT TREATEMENT. Limoges: University of Limoges, 2015.
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GAVENDOVÁ, P.; ČÍŽEK, J.; ČUPERA, J.; HASEGAWA, M.; DLOUHÝ, I. Microstructure modification of CGDS and HVOF sprayed CoNiCrAlY bond coat remelted by electron beam. New Methods of Damage and Failure Analysis of Structural Parts. VŠB-TU Ostrava. Ostrava: Vydavatelství VŠB-TU Ostrava, 2014. p. 119-120. ISBN: 978-80-248-3488-7.
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SEINER, H.; ČÍŽEK, J.; SEDLÁK, P.; HUANG, R.; ČUPERA, J.; DLOUHÝ, I.; LANDA, M. Elastic moduli and elastic anisotropy of cold sprayed metallic coatings. Surface and Coatings Technology, 2016, vol. 291, no. N/A, p. 342-347. ISSN: 0257-8972.
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ALIASGHARI, S.; NĚMCOVÁ, A.; ČÍŽEK, J.; GHOLINIA, A.; SKELDON, P.; THOMPSON, G. Effects of reagent purity on plasma electrolytic oxidation of titanium in an aluminate–phosphate electrolyte. TRANSACTIONS OF THE INSTITUTE OF METAL FINISHING, 2016, vol. 94, no. 1, p. 32-42. ISSN: 0020-2967.
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MORAVČÍK, I.; ČÍŽEK, J.; GAVENDOVÁ, P.; SHEIKH, S.; GUO, S.; DLOUHÝ, I. Effect of heat treatment on microstructure and mechanical properties of spark plasma sintered AlCoCrFeNiTi0.5 high entropy alloy. MATERIALS LETTERS, 2016, vol. 174, no. 1, p. 53-56. ISSN: 0167-577X.
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GAVENDOVÁ, P.; ČÍŽEK, J.; ČUPERA, J.; HASEGAWA, M.; DLOUHÝ, I. Microstructure modification of CGDS and HVOF sprayed CoNiCrAlY bond coat remelted by electron beam. Procedia Materials Science, 2016, vol. 12, no. 1, p. 89-94. ISSN: 2211-8128.
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MORAVČÍK, I.; ČÍŽEK, J.; DLOUHÝ, I.; KRAJŇÁKOVÁ, P. INFLUENCE OF SINTERING TEMPERATURE ON MICROSTRUCTURE AND HARDNESS OF AlCoCrFeNiTi0.5 HIGH ENTROPY ALLOY. In METAL 2016. Brno: TANGER Ltd., 2016. p. 64-65. ISBN: 978-80-87294-66-6.
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KHUN, N.; LI, Z.; KHOR, K.; ČÍŽEK, J. Higher in-flight particle velocities enhance in vitro tribological behavior of plasma sprayed hydroxyapatite coatings. Tribology International, 2016, vol. 103, no. 1, p. 496-503. ISSN: 0301-679X.
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MATĚJKOVÁ, M.; ČÍŽEK, J.; GEARTNER, F.; KLASSEN,; DLOUHÝ, I. Effect of processing parameters on high-energy ball milling HA/Ti composite powders. In Multi-scale design of advanced materials conference proceedings. 2016. p. 19-24. ISBN: 978-80-214-5358-6.
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ČUPERA, J. Imaging of lattice orientation and deformations by electron channelling contrast imaging compared with low voltage imaging and EBSD. In MULTI-SCALE DESIGN OF ADVANCED MATERIALS CONFERENCE PROCEEDINGS. Brno: Brno University of Technology, 2016. p. 2-12. ISBN: 978-80-214-5358-6.
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ČÍŽEK, J.; CÉNEK, L.; MATĚJKOVÁ, M.; KOUŘIL, J.; ČUPERA, J.; DLOUHÝ, I. Potential of New-Generation Electron Beam Technology in Interface Modification of Cold and HVOF Sprayed MCrAlY Bond Coats. In Proceedings of SMT30. Milan, Itálie: Politecnico di Milano, 2016. p. 1-5. ISBN: 9782123456803.
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ČÍŽEK, J.; SEINER, H.; SEDLÁK, P.; HUANG, R.; ČUPERA, J.; DLOUHÝ, I.; LANDA, M. Elastic moduli, isotropy, and deformation accommodation mechanisms of cold sprayed deposits. In Proceedings of NMDFSP. Yokohama: Yokohama National University, 2016. p. 3-4. ISBN: 9782123456803.
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YIN, S.; XIE, Y.; ČÍŽEK, J.; EMMANUEL, E.; TANVIR, H.; DOWLING, D.; LUPOI, R. Advanced diamond-reinforced metal matrix composites via cold spray: Properties and deposition mechanism. COMPOSITES PART B-ENGINEERING, 2017, vol. 113, no. 1, p. 44-54. ISSN: 1359-8368.
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KRAJŇÁKOVÁ, P.; DLOUHÝ, I.; ČÍŽEK, J.; ČUPERA, J.; SHVAB, R. Effect of Double Electron beam Remelting on Microstructure of HVOF and CGDS Bond Coat. In Metallography XVI. Materials Science Forum. Zurich, Switzerland: Trans tech Publications Ltd, 2017. p. 574-578. ISBN: 978-3-0357-1018-2. ISSN: 0255-5476.
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KRAJŇÁKOVÁ, P.; ČUPERA, J.; JAN, V.; DLOUHÝ, I. STUDY OF THE ELECTRON BEAM REMELTING OF A CGDS DEPOSITED CONICRALY LAYERS. In METAL 2017: 26TH INTERNATIONAL CONFERENCE ON METALLURGY AND MATERIALS. KELTICKOVA 62, SLEZSKA, OSTRAVA 710 00, CZECH REPUBLIC: TANGER LTD, 2017. p. 1333-1337. ISBN: 978-80-87294-79-6.
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HANUSOVÁ, P.; VODĚROVÁ, M. Vliv technologie zpracování na strukturu a vlastnosti slitiny Al - Fe - Ni. In SEMDOK 2014 19th International seminar of Ph.D. students. Žilina: 2014. s. 120-123. ISBN: 978-80-554-0832-3.
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Responsibility: Dlouhý Ivo, prof. Ing., CSc.