Publication detail

Optimization of the HS-SPME method coupled with GC/uECD for determination of methylmercury in water

KRÁLOVÁ, Z. VÁVROVÁ, M. ŠUCMAN, E. KOMÁRKOVÁ, P.

Original Title

Optimization of the HS-SPME method coupled with GC/uECD for determination of methylmercury in water

Type

journal article in Web of Science

Language

English

Original Abstract

The aim of this study was the optimization of the Solid Phase Micro-extraction (SPME) method and the optimization of gas chromatography using an electron capture detector method. The analytical procedure involves derivatization of ionic mercury with sodium tetraethylborate in a sample vial and following extraction with a silica polydimethylsiloxane coated fibre.

Keywords

methylmercury, solid phase micro-extraction, optimization, gas chromatography

Authors

KRÁLOVÁ, Z.; VÁVROVÁ, M.; ŠUCMAN, E.; KOMÁRKOVÁ, P.

RIV year

2014

Released

15. 12. 2014

ISBN

1018-4619

Periodical

Fresenius Environmental Bulletin

Year of study

23

Number

12B

State

Federal Republic of Germany

Pages from

3362

Pages to

3365

Pages count

4

BibTex

@article{BUT111051,
  author="Zuzana {Králová} and Milada {Vávrová} and Emanuel {Šucman} and Petra {Komárková}",
  title="Optimization of the HS-SPME method coupled with GC/uECD for determination of methylmercury in water",
  journal="Fresenius Environmental Bulletin",
  year="2014",
  volume="23",
  number="12B",
  pages="3362--3365",
  issn="1018-4619"
}