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KUNDRÁT, V. MATOUŠKOVÁ, P. MÁROVÁ, I.
Original Title
Facile Preparation of Porous Microfiber from Poly-3-(R)-Hydroxybutyrate and Its Application
Type
journal article in Web of Science
Language
English
Original Abstract
In this study, we described the development of a simplified wet spinning method of the production of a novel type of porous continuous fiber based on poly-3-(R)-hydroxybutyrate (PHB). The principle of this method is precipitation of PHB dissolved in chloroform solution into the ethanol precipitation bath. The influence of various PHB concentrations and feed rates on specific surface area (measured by nitrogen absorption method) was studied. Materials were also characterized by SEM. Surface areas of fibers achieved by wet spinning were in the range of tens of m(2).g(-1), and the biggest surface area value was 55 m(2).g(-1). The average diameter of fibers was in the range of 20-120 mu m and was dependent on both PHB concentration and feed rate. Optimum conditions for reaching stable fibers of high surface area were 3-5 % w.t. of PHB and feed rate 0.5-3 ml.h(-1). Fibers were functionalized by adsorption of some natural plant extracts. The incorporation of active substances into fibers was confirmed by infrared spectroscopy. High antioxidant and antimicrobial effect of PHB-fibers with cloves extract was found, as well as excellent long-term stability and optimal dynamics of the release of active compounds. The newly produced material would be applicable in pharmacy, cosmetics, and wound healing.
Keywords
P-3-HB; PHB; wet spinning; microfiber; pores
Authors
KUNDRÁT, V.; MATOUŠKOVÁ, P.; MÁROVÁ, I.
Released
20. 1. 2020
Publisher
MDPI
Location
BASEL
ISBN
1996-1944
Periodical
Materials
Year of study
13
Number
1
State
Swiss Confederation
Pages from
Pages to
14
Pages count
URL
https://doi.org/10.3390/ma13010086
Full text in the Digital Library
http://hdl.handle.net/11012/195648
BibTex
@article{BUT161667, author="Vojtěch {Kundrát} and Petra {Skoumalová} and Ivana {Márová}", title="Facile Preparation of Porous Microfiber from Poly-3-(R)-Hydroxybutyrate and Its Application", journal="Materials", year="2020", volume="13", number="1", pages="1--14", doi="10.3390/ma13010086", issn="1996-1944", url="https://doi.org/10.3390/ma13010086" }