Publication detail

Ex-situ Cell with Positioner for XRD Measurements in an Inert Atmosphere

KLVAČ, O. VYROUBAL, P. BAYER, R. ČECH, O.

Original Title

Ex-situ Cell with Positioner for XRD Measurements in an Inert Atmosphere

Type

conference paper

Language

English

Original Abstract

This paper describes the construction of a hermetically insulated cell for post-mortem research of electrode materials of electrochemical cells. The first part specifies the problems of XRD characterization, followed by a description of the cell solving problems with hermetic insulation and distortion of diffraction patterns. Then, a positioning system for sample displacement error correction is described and tested on the example of the Al2O3 powder standard. Finally, the measurement procedure using the constructed device on the example of a graphite electrode of the li-ion cell is shown.

Keywords

XRD, post-mortem, cell, intert atmospehre

Authors

KLVAČ, O.; VYROUBAL, P.; BAYER, R.; ČECH, O.

Released

11. 12. 2020

Publisher

IOP Publishing Ltd

ISBN

978-1-60768-909-6

Book

21st International Conference on Advanced Batteries,Accumulators and Fuel Cells (ABAF 2020)

ISBN

1938-6737

Periodical

ECS Transaction

Year of study

99

Number

1

State

United States of America

Pages from

333

Pages to

339

Pages count

7

URL

https://iopscience.iop.org/article/10.1149/09901.0333ecst/pdf

BibTex

@inproceedings{BUT167574,
  author="Ondřej {Klvač} and Petr {Vyroubal} and Robert {Bayer} and Ondřej {Čech}",
  title="Ex-situ Cell with Positioner for XRD Measurements in an Inert Atmosphere",
  booktitle="21st International Conference on Advanced Batteries,Accumulators and Fuel Cells (ABAF 2020)",
  year="2020",
  journal="ECS Transaction",
  volume="99",
  number="1",
  pages="333--339",
  publisher="IOP Publishing Ltd",
  doi="10.1149/09901.0333ecst",
  isbn="978-1-60768-909-6",
  issn="1938-6737",
  url="https://iopscience.iop.org/article/10.1149/09901.0333ecst/pdf"
}