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NEJDL, L. ZELNÍČKOVÁ, J. VANĚČKOVÁ, T. HYNEK, D. ADAM, V. VACULOVIČOVÁ, M.
Original Title
Rapid preparation of self-assembled CdTe quantum dots used for sensing of DNA in urine
Type
journal article in Web of Science
Language
English
Original Abstract
In this article, the authors report a systematic study of the self-assembly of CdTe quantum dots (QDs) stabilized by mercaptosuccinic acid (MSA) at laboratory temperature (25 degrees C) or after thermal treatment (90 degrees C). It was found that QD/MSA can be synthesized spontaneously under mild laboratory conditions (25 degrees C and 70 hours) without any further instrumentation or they can be treated using an increased temperature (90 degrees C and 8 min) to achieve the same fluorescence intensity. These QDs were used for the preparation of a fluorescent (off-on) probe based on methylene blue as a quencher for the specific determination of nucleic acid from urine. The whole process was monitored using stationary spectroscopy (absorbance and fluorescence measurement) and capillary electrophoresis (CE) with laser-induced fluorescence detection. The average size of the prepared QDs (approximately 3 nm) was determined using transmission electron microscopy and it was proven that the presented fluorescent probe combined with the CE method can be used for the sensitive determination of DNA (LOD 3 ng mL(-1)).
Keywords
CdTe quantum dots; DNA in urine
Authors
NEJDL, L.; ZELNÍČKOVÁ, J.; VANĚČKOVÁ, T.; HYNEK, D.; ADAM, V.; VACULOVIČOVÁ, M.
Released
21. 4. 2018
ISBN
1144-0546
Periodical
NEW JOURNAL OF CHEMISTRY
Year of study
42
Number
8
State
United Kingdom of Great Britain and Northern Ireland
Pages from
6005
Pages to
6012
Pages count
BibTex
@article{BUT149400, author="Lukáš {Nejdl} and Jaroslava {Zelníčková} and Tereza {Vaněčková} and David {Hynek} and Vojtěch {Adam} and Markéta {Vaculovičová}", title="Rapid preparation of self-assembled CdTe quantum dots used for sensing of DNA in urine", journal="NEW JOURNAL OF CHEMISTRY", year="2018", volume="42", number="8", pages="6005--6012", doi="10.1039/c7nj05167k", issn="1144-0546" }