Publication detail

THE DESIGN OF SAMPLE HOLDER FOR XRD MEASUREMENTS IN INERT ATMOSPHERE WITH DISPLACEMENT ERROR CORRECTION

KLVAČ, O.

Original Title

THE DESIGN OF SAMPLE HOLDER FOR XRD MEASUREMENTS IN INERT ATMOSPHERE WITH DISPLACEMENT ERROR CORRECTION

Type

conference paper

Language

English

Original Abstract

This article describes a designed of a holder for post-mortem XRD measurements of Li-ion, Na-ion and Li-S electrodes, which need to be performed in the inert atmosphere. The first part describes the measurement method and problems arising during the measurements of the samples. Subsequently, the design and construction of a new cell with hermetic insulation and sample displacement error correction possible during the operation of the diffractometer is described. Finally, the inert gas attenuation within the cell is theoretically calculated. The calculation is verified by practical measurements, and alternatives are proposed to improve the signal-to-noise ratio.

Keywords

XRD, ex-situ, post-mortem, sample displacement, attenuation, SNR

Authors

KLVAČ, O.

Released

23. 4. 2020

ISBN

978-80-214-5868-0

Book

Proceedings of the 26th Conference STUDENT EEICT 2020 Selected Papers

Edition

1

Edition number

25

Pages from

103

Pages to

107

Pages count

5

BibTex

@inproceedings{BUT166188,
  author="Ondřej {Klvač}",
  title="THE DESIGN OF SAMPLE HOLDER FOR XRD MEASUREMENTS IN INERT ATMOSPHERE WITH DISPLACEMENT ERROR CORRECTION",
  booktitle="Proceedings of the 26th Conference STUDENT EEICT 2020 Selected Papers",
  year="2020",
  series="1",
  number="25",
  pages="103--107",
  isbn="978-80-214-5868-0"
}