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BARTONÍČKOVÁ, E. CIHLÁŘ, J.
Original Title
Synthesis and processing of InVO4
Type
journal article - other
Language
English
Original Abstract
Indium vanadates for severe applications as photocatalysts, anodes for Li rechargeable batteries or electrochromic devices were prepared via conventional and non-conventional preparation methods. The conventional high temperature solid state reaction was performed at 800 C for 25 hours and the non-conventional microwave-assisted synthesis was performed at 220 C for different reaction times under hydrothermal conditions. The as-prepared powders were characterized in terms of phase composition by X-Ray diffraction analysis (XRD) and infrared spectroscopy (IR) and of powder morphology by scanning electron microscopy (SEM) and BET method. Nanosized indium vanadate powders were successfully synthesized by non-conventional microwave-assisted hydrothermal method. The dense ceramic bodies suitable for electrical conductivity measurements with 96% t.d. were obtained by sintering of powders prepared by high-temperature solid state reaction at 1100 C for 4 h with admission of oleic acid as a binder additive
Keywords
Indium vanadate; microwave-assisted hydrothermal synthesis
Authors
BARTONÍČKOVÁ, E.; CIHLÁŘ, J.
RIV year
2010
Released
8. 1. 2010
Publisher
WORLD SCIENTIFIC PUBL CO PTE LTD
Location
5 TOH TUCK LINK, SINGAPORE 596224, SINGAPORE
ISBN
0217-9792
Periodical
INTERNATIONAL JOURNAL OF MODERN PHYSICS B
Year of study
24
Number
6-7
State
Republic of Singapore
Pages from
770
Pages to
779
Pages count
10
BibTex
@article{BUT49500, author="Eva {Bartoníčková} and Jaroslav {Cihlář}", title="Synthesis and processing of InVO4", journal="INTERNATIONAL JOURNAL OF MODERN PHYSICS B", year="2010", volume="24", number="6-7", pages="770--779", issn="0217-9792" }