Course detail

Methods of structure analysis

FCH-MCT_MSAAcad. year: 2011/2012

Overwiev of structural organic analysis. Ultra-violet and infra-red spectroscopy. Nuclear magnetic resonance of 1H and 13C nucleus. Mass spectrometry.

Language of instruction

Czech

Number of ECTS credits

2

Mode of study

Not applicable.

Guarantor

prof. RNDr. Zdeněk Friedl, CSc.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Learning outcomes of the course unit

Completing the course students acquire the complex knowledge of interpreting spectra related to the structural organic analysis. The knowledge acquired enables to work both in research and practice of bioorganic and pharmaceutical chemistry, control laboratories and state administration authorities.

Prerequisites

Fundamentals of Organic chemistry I+II, Analytical chemistry II, practice from instrumental analytical chemistry.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

Teaching methods depend on the type of course unit as specified in the article 7 of BUT Rules for Studies and Examinations.

Assesment methods and criteria linked to learning outcomes

Completing the course proceeds in the form of graded credit.

Course curriculum

1. Ultraviolet spectroscopy. 2. Infrared spectroscopy. 3. Fundamentals of nuclear magnetic resonance spectroscopy. 4. 1D NMR 1H spectroscopy. 5. 1D NMR 13C spectroscopy. 6. Methods of 2D NMR spectroscopy. 7. NMR spectra of selected groups of organic compounds. 8. Fundamentals of mass spectrometry. 9. Mass spectra of selected groups of organic compounds. 10. Principles of structural organic analysis. 11-13. Practical solution of organic structural analysis based on spectra interpretation.

Work placements

Not applicable.

Aims

Acquirement of physical backgrounds of structural analytical methods. Ability to interpret experimental spectra with regard to structure elucidation of organic compounds.

Specification of controlled education, way of implementation and compensation for absences

The control of lectures is not given.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Böhm S.: Strukturní analýza organických sloučenin. VŠCHT v Praze, Praha 1995. (CS)

Recommended reading

Not applicable.

Classification of course in study plans

  • Programme NPCP_CHTOZP Master's

    branch NPCO_CHTOZP , 2 year of study, summer semester, compulsory-optional
    branch NPCO_CHTOZP , 1 year of study, summer semester, compulsory-optional

  • Programme NPCP_CHTP Master's

    branch NPCO_CHTP , 2 year of study, summer semester, compulsory-optional
    branch NPCO_CHTP , 1 year of study, summer semester, compulsory-optional

  • Programme NPCP_CHM Master's

    branch NPCO_CHM , 2 year of study, summer semester, compulsory-optional
    branch NPCO_CHM , 1 year of study, summer semester, compulsory-optional

  • Programme NPCP_SCH Master's

    branch NPCO_SCH , 2 year of study, summer semester, compulsory-optional
    branch NPCO_SCH , 1 year of study, summer semester, compulsory-optional

  • Programme CKCP_CZV lifelong learning

    branch CKCO_CZV , 1 year of study, summer semester, compulsory-optional

  • Programme NKCP_CHTOZP Master's

    branch NKCO_CHTOZP , 1 year of study, summer semester, compulsory-optional
    branch NKCO_CHTOZP , 2 year of study, summer semester, compulsory-optional

  • Programme NKCP_CHTP Master's

    branch NKCO_CHTP , 1 year of study, summer semester, compulsory-optional
    branch NKCO_CHTP , 2 year of study, summer semester, compulsory-optional

  • Programme NKCP_CHM Master's

    branch NKCO_CHM , 1 year of study, summer semester, compulsory-optional
    branch NKCO_CHM , 2 year of study, summer semester, compulsory-optional

  • Programme NKCP_SCH Master's

    branch NKCO_SCH , 1 year of study, summer semester, compulsory-optional
    branch NKCO_SCH , 2 year of study, summer semester, compulsory-optional

Type of course unit

 

Lecture

26 hod., optionally

Teacher / Lecturer

prof. Ing. Josef Čáslavský, CSc.
prof. RNDr. Zdeněk Friedl, CSc.

Guided consultation in combined form of studies

13 hod., optionally

Teacher / Lecturer

prof. RNDr. Zdeněk Friedl, CSc.