Course detail

Experimental Laboratory Methods

FAST-CJ03Acad. year: 2011/2012

The contents of the subject is a survey of common and special laboratory methods and of instrumentation techniques used in the silicate industry concentrated to the branches of ceramics, refractory and binding materials. The matter includes methods used in the technology of production, checking of raw materials from the point of view of their applicability in the technological process and the testing the properties of readymade products. The student deepens his knowledge in commonly performed laboratory tests and he becomes acquainted with special methods such as high pressure mercury porosimetry, X-ray diffraction, differential- thermal - analysis, optical microscopy and scanning electron microscopy. Attention is paid even to methods of the degradation determination of building materials.

Language of instruction

Czech

Number of ECTS credits

5

Mode of study

Not applicable.

Department

Institute of Technology of Building Materials and Components (THD)

Learning outcomes of the course unit

The student would manage the goal of the subject by acquiring knowledge and overview of common and special laboratory methods and equipment used in silicate industry, mainly in the production of construction substances and components.

Prerequisites

Theoretical fundamentals of silicates structure and chemistry, fundamentals of production technology and properties of building materials based on silicates, such as binders, ceramics, concrete etc.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

Not applicable.

Assesment methods and criteria linked to learning outcomes

Requirements for successful completion of the subject are specified by guarantor’s regulation updated for every academic year.

Course curriculum

1.Familiarization with the subject content, survey of laboratory methods in the branch of silicates.
2.Sampling, preparation and treatment of samples for individual methods.
3.X-ray diffraction analysis, apparatuses, principle and utilization.
4.Microscopy in the range of the visible spectrum, apparatuses, principle and preparations.
5.Electron transmission microscopy, principle, apparatuses, utilization.
6.Scanning electron microscopy, principle, apparatuses, utilization.
7.Methods of grain size and specific surface determination.
8.Methods of density, volume mass and absorption determination.
9.High pressure mercury porozimetry, principle, apparatuses, utilization.
10.Differential thermal analysis, principle apparatuses, utilization.
11.Gravimetric thermal analysis, principle, utilization.
12.Contraction dilatometric thermal analysis, principle, utilization.
13.Principles of building materials testing, quality control, harmonization of 13standards and regulations.

Work placements

Not applicable.

Aims

Obtaining knowledge concerning common and special laboratory methods and measuring, instruments used in silicate industry and especially in production of building materials and components, utilization of these methods for evaluation of raw materials suitability for building materials production and for determination of physico-mechanical and technological properties of readymade products

Specification of controlled education, way of implementation and compensation for absences

Extent and forms are specified by guarantor’s regulation updated for every academic year.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Šašek L. a kol.: Laboratorní metody v oboru silikátů. SNTL Praha, 1981. ISBN 80-7252-057-11. (CS)

Recommended reading

Dobrý O., Palek L: Koroze betonu ve stavební praxi, SNTL, 1988,. SNTL, 1988. ISBN 80-214-1158-1. (CS)
Experimentální laboratorní metody. (CS)
Lach, V., Daňková, M: Mikrostruktura stavebních látek. SNTL, 1999. (CS)

Classification of course in study plans

  • Programme N-P-E-SI Master's

    branch M , 1 year of study, winter semester, compulsory

  • Programme N-P-C-SI Master's

    branch M , 1 year of study, winter semester, compulsory

  • Programme N-K-C-SI Master's

    branch M , 1 year of study, winter semester, compulsory

Type of course unit

 

Lecture

26 hod., optionally

Teacher / Lecturer

Exercise

26 hod., compulsory

Teacher / Lecturer