Course detail

Laboratory Classes in Instrumental and Structure Analysis - CTEP

FCH-MC_ISA_ZAcad. year: 2023/2024

Practical class to the subject "Instrumental and Structure Analysis" - familiarization with instrumental analytical techniques applied in environmental analysis and technical praxis.

Language of instruction

Czech

Number of ECTS credits

3

Mode of study

Not applicable.

Entry knowledge

Good knowledge of common, inorganic, organic, physical and analytical chemistry

Rules for evaluation and completion of the course

Graded credit based on the submission of protocols from individual tasks. The final score is the average from scores for each protocol.
Attendance at practices is mandatory. For the credit awars it is essential to completing all tasks.

Aims

The aim of this subject is:
- to deepen the knowledge gained within the course of Instrumental and structural analysis
- to familiarize students with the methods of instrumental and structural analysis exploited in analytical practice.
Completion of this course will increase students' competence as follows:
1. Students will be acquainted with instrumental analytical methods used in analytical practice
2. Students will understand the capabilities and limitations of instrumental analytical methods
3. Students will be able to choose the optimal instrumental analytical method for solving a particular analytical problem.

Study aids

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Klouda P.: Moderní analytické metody. Nakladatelství Pavel Klouda, Ostrava 2003. (CS)

Recommended reading

Not applicable.

Elearning

Classification of course in study plans

  • Programme NPCP_ECHT Master's 1 year of study, winter semester, compulsory
  • Programme NKCP_ECHT Master's 1 year of study, winter semester, compulsory

Type of course unit

 

Guided consultation in combined form of studies

26 hod., optionally

Teacher / Lecturer

Laboratory exercise

39 hod., compulsory

Teacher / Lecturer

Syllabus

1. Informative meeting about subject organization
2. Spectrophotometry - UV-VIS
3. Infrared spectrometry - IR
4. Atomic absorption spectrometry - AAS
5. Inductively coupled plasma-mass spectrometry - ICP-MS
6. Inductively coupled plasma-optical emission spectrometry - ICP-OES
7. Gas chromatography with flame ionization - GC/FID
8. Gas chromatography with mass spectrometric detection - GC/MS
9. Reversed-phase liquid chromatography - HPLC/DAD
10. Isotachophoresis
11. Liquid chromatography with mass spectrometric detection - LC/MS
12. Differential compensation calorimetry - DSC
13. Thermal gravimetric analysis - TGA

Elearning