Přístupnostní navigace
E-přihláška
Vyhledávání Vyhledat Zavřít
Detail publikace
DIVIŠOVÁ, R. VÍTOVÁ, E. DIVIŠ, P. ZEMANOVÁ, J. OMELKOVÁ, J.
Originální název
Validation of SPME–GC–FID Method for Determination of Fragrance Allergens in Selected Cosmetic Products
Typ
článek v časopise ve Web of Science, Jimp
Jazyk
angličtina
Originální abstrakt
An analytical method for simultaneous determination of 24 legislatively restricted fragrance allergens in various cosmetic products was developed and validated using a combination of solid-phase microextraction and gas chromatography with flame ionization detector. The divinylbenzene-polydimethylsiloxane (DVB-PDMS) fiber was evaluated as the best for extraction of all studied fragrance allergens at 40oC and 20 min extraction time. All calibration curves showed good linearity in the range of 10-1 to 103 ug mL-1. Good repeatability and inter-day precision was determined for the proposed method. Detection limits for individual allergens ranged from 0.007 to 2.7 ug mL-1. The validated method was used to analyze real cosmetic samples. The obtained results indicated that not all of the analyzed cosmetic samples were labeled in accordance with European Cosmetic Directive.
Klíčová slova
SPME, GC, fragrances, cosmetics
Autoři
DIVIŠOVÁ, R.; VÍTOVÁ, E.; DIVIŠ, P.; ZEMANOVÁ, J.; OMELKOVÁ, J.
Rok RIV
2015
Vydáno
5. 1. 2015
ISSN
1233-2356
Periodikum
ACTA CHROMATOGRAPHICA
Ročník
27
Číslo
3
Stát
Polská republika
Strany od
509
Strany do
523
Strany počet
15
URL
https://akademiai.com/doi/pdf/10.1556/AChrom.27.2015.3.8
BibTex
@article{BUT113399, author="Radka {Divišová} and Eva {Vítová} and Pavel {Diviš} and Jana {Zemanová} and Jiřina {Omelková}", title="Validation of SPME–GC–FID Method for Determination of Fragrance Allergens in Selected Cosmetic Products", journal="ACTA CHROMATOGRAPHICA", year="2015", volume="27", number="3", pages="509--523", doi="10.1556/AChrom.27.2015.3.8", issn="1233-2356", url="https://akademiai.com/doi/pdf/10.1556/AChrom.27.2015.3.8" }