Detail publikace

Evaluating the suitability of fast sintering techniques for the consolidation of calcium phosphate scaffolds produced by DLP

PAREDES SÁNCHEZ, C. ROLEČEK, J. PEJCHALOVÁ, L. SPUSTA, T. SALAMON, D. MIRANDA, P.

Originální název

Evaluating the suitability of fast sintering techniques for the consolidation of calcium phosphate scaffolds produced by DLP

Typ

článek v časopise ve Web of Science, Jimp

Jazyk

angličtina

Originální abstrakt

Porous scaffolds were fabricated via Digital Light Processing (DLP) from beta-TCP powder and sintered by conventional sintering in air (CSA), rapid sintering in air (RSA) and pressure-less spark plasma sintering in vacuum (pl-SPS), at four different temperatures: 1200, 1300, 1400 and 1500 degrees C. Each sintering strategy resulted in scaffolds with different phase composition, microstructure and mechanical properties. Long dwell times or high temperatures were required to achieve a complete beta ->alpha transformation, and rapid cooling rates avoided the reverse transformation. The presence of graphite in the sintering chamber played a crucial role in stabilising the alpha-TCP phase, phase prevailing in SPS-treated scaffolds, hindered their densification and avoided the generation of transformation-induced cracks. All scaffolds exhibited compressive strengths within the range of cancellous bone, with the highest average value of 22 +/- 4 MPa achieved by the RSA scaffolds sintered at 1300 degrees C, thanks to their greater densification and fine microstructure.

Klíčová slova

Scaffolds; Calcium phosphate; Mechanical properties; Digital Light Processing; Spark Plasma Sintering

Autoři

PAREDES SÁNCHEZ, C.; ROLEČEK, J.; PEJCHALOVÁ, L.; SPUSTA, T.; SALAMON, D.; MIRANDA, P.

Vydáno

1. 11. 2023

Nakladatel

ELSEVIER SCI LTD

Místo

OXFORD

ISSN

1873-619X

Periodikum

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY

Ročník

43

Číslo

14

Stát

Spojené království Velké Británie a Severního Irska

Strany od

6493

Strany do

6503

Strany počet

11

URL

https://www.sciencedirect.com/science/article/pii/S0955221923004272?via%3Dihub

Plný text v Digitální knihovně

http://hdl.handle.net/11012/245109

BibTex

@article{BUT185512,
  author="Claudia Isabel {Paredes Sánchez} and Jakub {Roleček} and Lucie {Mařáková} and Tomáš {Spusta} and David {Salamon} and Pedro {Miranda}",
  title="Evaluating the suitability of fast sintering techniques for the consolidation of calcium phosphate scaffolds produced by DLP",
  journal="JOURNAL OF THE EUROPEAN CERAMIC SOCIETY",
  year="2023",
  volume="43",
  number="14",
  pages="6493--6503",
  doi="10.1016/j.jeurceramsoc.2023.05.052",
  issn="1873-619X",
  url="https://www.sciencedirect.com/science/article/pii/S0955221923004272?via%3Dihub"
}