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Publication detail
J.Špinka, J.Jirák
Original Title
X - RAY MICROANALYSIS IN ESEM
Type
conference paper
Language
English
Original Abstract
The X-ray microanalysis performed in ESEM requires to take into account presence of gas in the specimen chamber. The impact of electron scattering causes disadvantageous general increase of concentration limits of executed analysis by additional X-ray peaks contributed by the so called skirt. At X-ray analysis scattered skirt electrons interact with atoms of specimen and produce X-rays but we do not know which X-rays are produced by primary beam and which are produced by skirt electrons. Pressure variation method is described. This method enables extrapolation of X- ray spectral measurements at higher pressures to zero pressure.
Keywords
ESEM, X-ray, microanalysis
Authors
RIV year
2006
Released
30. 4. 2006
Publisher
TU Brno, Department of Electrotechnolgy
Location
Brno
ISBN
80-214-3181-4
Book
7th Aba BRNO 2006
Pages from
153
Pages to
156
Pages count
4
BibTex
@inproceedings{BUT21694, author="Jiří {Špinka} and Josef {Jirák}", title="X - RAY MICROANALYSIS IN ESEM", booktitle="7th Aba BRNO 2006", year="2006", pages="4", publisher="TU Brno, Department of Electrotechnolgy", address="Brno", isbn="80-214-3181-4" }