Course detail

Laboratory Classes in Analytical Chemistry II

FCH-BCA_ANC2_PAcad. year: 2011/2012

Practical training at selected basic instrumental analytical methods: potentiometry, automatic titrations, spectrophotometry, fluorimetry, emission flame photometry, thin-layer chromatography, ionex chromatography, electrogravimetry

Language of instruction

Czech

Number of ECTS credits

5

Mode of study

Not applicable.

Guarantor

prof. Ing. Josef Čáslavský, CSc.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Learning outcomes of the course unit

Introduction to selected analytical procedures and methods.
Evaluation of results, obtaining skills essential for experimentation, sample handling according to GLP.
Practising of calculations used in analytical chemistry

Prerequisites

Laboratory course of analytical chemistry I.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

Teaching methods depend on the type of course unit as specified in the article 7 of BUT Rules for Studies and Examinations.

Assesment methods and criteria linked to learning outcomes

Graded course-unit credit
Requirements:
- all laboratory tasks completed, results and reports in good quality
- course test
Final classification is based on average classification of individual tasks.

Course curriculum

Redox and potentiometric titrations
Potentiometric titrations (precipitation titrations)
Automatic acid-base titrations
Titrations in nonaqueous solvents
Spectrophotometry
Spectrophotometry in mixtures
Extraction spectrometry
Fluorimetry
Emission spectroscopy
Chromatographic methods (TLC, IEC)
Analysis of copper-based alloys

Work placements

Not applicable.

Aims

Familiarization with the basic instrumental methods used in analytical chemistry.

Specification of controlled education, way of implementation and compensation for absences

Written entrance tests at the beginning of all exercises checking the students readiness for practical work.
Credit test at the course end.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Šimek Z., Komendová R., Mašek I., Voznica P. : Kvantitativní analýza. FCH VUT v Brně, Brno 2003. (CS)

Recommended reading

Sommer L. : Základy analytické chemie I. VUTIUM, Brno 1998. (CS)
Sommer L. a kol. : Základy analytické chemie II. VUTIUM, Brno 2000. (CS)
Vláčil F. a kol. : Příklady z chemické a instumentální analýzy. INFORMATORIUM, Praha 1991. (CS)

Classification of course in study plans

  • Programme BPCP_CHCHT Bachelor's

    branch BPCO_CHTOZP , 2 year of study, summer semester, compulsory
    branch BPCO_CHM , 2 year of study, summer semester, compulsory
    branch BPCO_SCH , 2 year of study, summer semester, compulsory

  • Programme BPCP_CHTP Bachelor's

    branch BPCO_CHP , 2 year of study, summer semester, compulsory

  • Programme BPCP_CHCHT Bachelor's

    branch BPCO_CHMN , 2 year of study, summer semester, compulsory

  • Programme BPCP_CHTP Bachelor's

    branch BPCO_BT , 2 year of study, summer semester, compulsory

  • Programme CKCP_CZV lifelong learning

    branch CKCO_CZV , 1 year of study, summer semester, compulsory

  • Programme BKCP_CHCHT Bachelor's

    branch BKCO_CHTOZP , 2 year of study, summer semester, compulsory
    branch BKCO_SCH , 2 year of study, summer semester, compulsory
    branch BKCO_CHM , 2 year of study, summer semester, compulsory

  • Programme BKCP_CHTP Bachelor's

    branch BKCO_PCH , 2 year of study, summer semester, compulsory
    branch BKCO_BT , 2 year of study, summer semester, compulsory

Type of course unit

 

Laboratory exercise

65 hod., compulsory

Teacher / Lecturer

Ing. Josef Kotlík, CSc.
doc. Mgr. Renata Komendová, Ph.D.