Course detail

Laboratory Classes in Analytical Chemistry II

FCH-BAA_ANC2_PAcad. year: 2012/2013

Practical training at selected basic instrumental analytical methods: potentiometry, automatic titrations, spectrophotometry, fluorimetry, emission flame photometry, thin-layer chromatography, ionex chromatography, electrogravimetry

Language of instruction

English

Number of ECTS credits

5

Mode of study

Not applicable.

Guarantor

prof. Ing. Josef Čáslavský, CSc.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Offered to foreign students

Of all faculties

Learning outcomes of the course unit

Introduction to selected analytical procedures and methods.
Evaluation of results, obtaining skills essential for experimentation, sample handling according to GLP.
Practising of calculations used in analytical chemistry

Prerequisites

Laboratory Classes in Analytical chemistry I.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

Teaching methods depend on the type of course unit as specified in the article 7 of BUT Rules for Studies and Examinations.

Assesment methods and criteria linked to learning outcomes

Graded course-unit credit
Requirements:
- all laboratory tasks completed, results and reports in good quality
- course test

Course curriculum

Redox titrations with potentiometric indication
Potentiometric titrations (precipitation titrations)
Automatic acid-base titrations
Titrations in nonaqueous solvents
Spectrophotometry
Spectrophotometry in mixtures
Extraction spectrometry
Fluorimetry
Emission spectroscopy
Chromatographic methods (TLC, IEC)
Analysis of copper-based alloys

Work placements

Not applicable.

Aims

Familiarization with the basic instrumental methods used in analytical chemistry.

Specification of controlled education, way of implementation and compensation for absences

Written entrance tests at the beginning of all exercises checking the students readiness for practical work.
Credit test at the course end.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Z.Šimek et al.: Quantitative analysis (EN)

Recommended reading

Not applicable.

Classification of course in study plans

Type of course unit

 

Laboratory exercise

78 hod., compulsory

Teacher / Lecturer

prof. Ing. Josef Čáslavský, CSc.